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Chemical analysis : modern instrumentation methods and techniques / Francis Rouessac, Annick Rouessac; translated by Francis and Annick Rouessac, Steve Brooks

Main Author Rouessac, Francis Coauthor Rouessac, Annick Secondary Author Brooks, Steve Country Reino Unido. Edition 2nd ed Publication Chichester : John Wiley & Sons, cop. 2007 Description XXIII, 574 p. : il. ; 25 cm ISBN 978-0-470-85903-2 CDU 543
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Holdings
Item type Current location Call number Status Date due Barcode Item holds Course reserves
Monografia Biblioteca de Engenharia Biológica
BEB 543 - R Indisponível | Not available 371600

Mestrado Integrado em Engenharia Biológica Laboratórios de Tecnologia Química 1º semestre

Mestrado Integrado em Engenharia Biológica Laboratórios de Bioprocessos 2º semestre

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Enhanced descriptions from Syndetics:

Completely revised and updated, Chemical Analysis: Second Edition is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through the more widely used and important techniques, whilst avoiding excessive technical detail. Provides a thorough introduction to a wide range of the most important and widely used instrumental techniques Maintains a careful balance between depth and breadth of coverage Includes examples, problems and their solutions Includes coverage of latest developments including supercritical fluid chromatography and capillary electrophoresis

Table of contents provided by Syndetics

  • Foreword to the first English edition
  • Preface to the first English edition
  • Preface to second edition
  • Acknowledgments
  • Introduction
  • Part 1 Separation Methods
  • 1 General aspects of chromatography
  • 1.1 General concepts of analytical chromatography
  • 1.2 The chromatogram
  • 1.3 Gaussian-shaped elution peaks
  • 1.4 The plate theory
  • 1.5 Nernst partition coefficient (K)
  • 1.6 Column efficiency
  • 1.7 Retention parameters
  • 1.8 Separation (or selectivity) factor between two solutes
  • 1.9 Resolution factor between two peaks
  • 1.10 The rate theory of chromatography
  • 1.11 Optimization of a chromatographic analysis
  • 1.12 Classification of chromatographic techniques
  • Problems 2
  • 2.1 Components of a GC installation
  • 2.2 Carrier gas and flow regulation
  • 2.3 Sample introduction and the injection chamber
  • 2.4 Thermostatically controlled oven
  • 2.5 Columns
  • 2.6 Stationary phases
  • 2.7 Principal gas chromatographic detectors
  • 2.8 Detectors providing structural data
  • 2.9 Fast chromatography
  • 2.10 Multi-dimensional chromatography
  • 2.11 Retention indexes and stationary phase constants
  • Problems. 3 High-performance liquid chromatography
  • 3.1 The beginnings of HPLC
  • 3.2 General concept of an HPLC system
  • 3.3 Pumps and gradient elution
  • 3.4 Injectors
  • 3.5 Columns
  • 3.6 Stationary phases
  • 3.7 Chiral chromatography
  • 3.8 Mobile phases
  • 3.9 Paired-ion chromatography
  • 3.10 Hydrophobic interaction chromatography
  • 3.11 Principal detectors
  • 3.12 Evolution and applications of HPLC
  • Problems. 4 Ion chromatography
  • 4.1 Basics of ion chromatography
  • 4.2 Stationary phases
  • 4.3 Mobile phases
  • 4.4 Conductivity detectors
  • 4.5 Ion suppressors
  • 4.6 Principle and basic relationship
  • 4.7 Areas of the peaks and data treatment software
  • 4.8 External standard method
  • 4.9 Internal standard method
  • 4.10 Internal normalization method
  • Problems. 5 Thin layer chromatography
  • 5.1 Principle of TLC
  • 5.2 Characteristics of TLC
  • 5.3 Stationary phases
  • 5.4 Separation and retention parameters
  • 5.5 Quantitative TLC
  • Problems. 6 Supercritical fluid chromatography
  • 6.1 Supercritical fluids: a reminder
  • 6.2 Supercritical fluids as mobile phases
  • 6.3 Instrumentation in SFC
  • 6.4 Comparison of SFC with HPLC and GC
  • 6.5 SFC in chromatographic techniques
  • 7 Size exclusion chromatography
  • 7.1 Principle of SEC
  • 7.2 Stationary and mobile phases
  • 7.3 Calibration curves
  • 7.4 Instrumentation
  • 7.5 Applications of SEC
  • Problems. 8 Capillary electrophoresis and electrochromatography
  • 8.1 From zone electrophoresis to capillary electrophoresis
  • 8.2 Electrophoretic mobility and electro-osmotic flow
  • 8.3 Instrumentation
  • 8.4 Electrophoretic techniques
  • 8.5 Performance of CE
  • 8.6 Capillary electrochromatography
  • Problems
  • Part 2 Spectroscopic Methods
  • 9 Ultraviolet and visible absorption spectroscopy
  • 9.1 The UV/Vis spectral region and the origin of the absorptions
  • 9.2 The UV/Vis spectrum
  • 9.3 Electronic transitions of organic compounds
  • 9.4 Chromophore groups
  • 9.5 Solvent effects: solvatochromism
  • 9.6 Fieser-Woodward rules
  • 9.7 Instrumentation in the UV/Visible
  • 9.8 UV/Vis spectrophotometers
  • 9.9 Quantitative analysis

Author notes provided by Syndetics

Francis Rouessac is the author of Chemical Analysis: Modern Instrumentation Methods and Techniques, 2nd Edition, published by Wiley.

Annick Rouessac is the author of Chemical Analysis: Modern Instrumentation Methods and Techniques, 2nd Edition, published by Wiley.

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